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This book contains a novel combination of experimental§and model-based investigations, elucidating the complex processes inside zinc§air batteries. The work presented helps to answer which battery composition and§which air-composition should be adjusted to maintain stable and efficient§charge/discharge cycling.§In detail, electrochemical investigations and X-ray§transmission tomography are applied on button cell zinc air batteries and§in-house set-ups. Moreover, model-based investigations of the battery anode and§the impact of relative humidity, active operation, carbon dioxide and oxygen on§zinc air battery operation are presented. The§techniques used in this work complement each other well and yield an unprecedented understanding of zinc air§batteries. The methods applied are adaptable and can potentially be applied to§gain further understanding of other metal air batteries.§